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YANG Chao, YANG Wei-cheng, LI Mei-hua, LUO Yong. Syntheses of Stable Isotope Labeled D12-Malachite Green[J]. Journal of Isotopes, 2014, 27(2): 77-81. DOI: 10.7538/tws.2014.27.02.0077
Citation: YANG Chao, YANG Wei-cheng, LI Mei-hua, LUO Yong. Syntheses of Stable Isotope Labeled D12-Malachite Green[J]. Journal of Isotopes, 2014, 27(2): 77-81. DOI: 10.7538/tws.2014.27.02.0077
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Syntheses of Stable Isotope Labeled D12-Malachite Green

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  • The efficient synthesis of stable isotope labeled D12-Malachite Green with CD3OD as the precursor by methylation, condensation and oxidation was presented. The yields of D12-Malachite Green was 50.1 % based on CD3OD consumed. The product was ideatified by HPLC, MS, and NMR to be the target compound. Its chemical purity and isotopic enrichment were higher than 99.0 atom%D. The result showed that the D12-Malachite Green could be used as internal standard in the field of food safety.
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