Investigation and Comparison of ~3He Cleanup Methods
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摘要: 报道了采用 70 0℃铀床、77K低温活性炭柱提取高纯 3He,之后采用氢同位素稀释法除去 3He中微量氚的研究结果。 70 0℃流通式铀床和 77K低温活性炭柱吸附方法, 能快速除去 3He中杂质组分, 得到纯度大于 99.99%的高纯 3He;氢同位素稀释法能够将 3He中 3H摩尔分数降到低于 3.5×10 -10 %。与其他方法比较, 氢同位素稀释法工艺过程更加简单, 3He收率更高Abstract: He cleanup methods using uranium bed and active carbon absorption and then using hydrogen isotope dilution to elimination trace tritium are introduced. The results show that both U bed and active carbon absorption column are effective in 3He extraction. 3He gas with purity 99.99% is obtained using these methods and 3H mole fraction in 3He is reduced dowm to 3.5×10 -10 % using hydrogen isotope dilution. Comparing with the other methods, the U bed and hydrogen isotope dilution methods are more effective and simple in 3He cleanup and trace tritium elimination.
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Keywords:
- ~3He /
- cleanup /
- active carbon absorption /
- uranium bed /
- hydrogen isotope dilution method
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[1] Poitras JP.Tritium Remove From Gasses[R].ML M- 1389. 1967. [2] Wong KY,Hirircq B,Jalbert RA.Tritium Decontamination of Machine Components and Walls[J].Fusion Engineering and Design,1991,2 1:159~ 172. [3] 张伟, 陶精言.氚的生产 [M].北京: 原子能工业出版社, 1980
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