冻干人尿碘成份分析标准物质中碘的超热中子活化定值分析

  • 摘要: 用超热中子活化分析法(ENAA)对两种冻干人尿碘成份分析标准物质中碘元素的含量进行了定值,该方法的灵敏度比全堆谱中子活化分析法(TNAA)提高了一个数量级,十次测量结果的相对标准偏差分别为2.9%和3.3%。为检验分析数据的可靠性,同时对研制单位提供的两种质控样品进行了分析,测量结果的平均值与给出值吻合很好,相对误差小于3%。

     

    Abstract: ENAA OF IODINE IN STANDARD REFERENCE MATERIAL LYOPHILIZED HUMAN URINEZhang Yongbao Wang Ke(China Institute of Atomic Energy, Beijing 102413)Wang Ganfeng(China Institute of Occupational Medicine, Beijing 100050)ABSTRACTThe contents of iodine in two kinds of standard reference materials lyophilized human urine are determined by ENAA. The sensitivity of this method is ten times higher than that of TNAA, and the relative standard deviations of ten measurements are 2.9% and 3.3%, respectively. Two certificated reference samples are used for verification of the analysis. The analytical results are in agreement with the recommended values, and the relative error is less than 3%.Key words lyophilized human urine standard reference material iodine epithermal neutron activation analysis(ENAA)

     

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